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Accuracy in the experimental calorimetric study of the crystallization kinetics and predicitve transformation diagrams: Application to a Ga-Te amorphous alloy

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dc.creator Clavaguera, N. (Clavaguera Plaja)
dc.creator Clavaguera-Mora, M. T.
dc.creator Fontana, M.
dc.date 2011-05-25T10:53:58Z
dc.date 2011-05-25T10:53:58Z
dc.date 1998
dc.date.accessioned 2024-12-16T10:27:07Z
dc.date.available 2024-12-16T10:27:07Z
dc.identifier 0884-2914
dc.identifier http://hdl.handle.net/2445/18198
dc.identifier 127055
dc.identifier.uri http://fima-docencia.ub.edu:8080/xmlui/handle/123456789/21911
dc.description The uncertainties inherent to experimental differential scanning calorimetric data are evaluated. A new procedure is developed to perform the kinetic analysis of continuous heating calorimetric data when the heat capacity of the sample changes during the crystallization. The accuracy of isothermal calorimetric data is analyzed in terms of the peak-to-peak noise of the calorimetric signal and base line drift typical of differential scanning calorimetry equipment. Their influence in the evaluation of the kinetic parameters is discussed. An empirical construction of the time-temperature and temperature heating rate transformation diagrams, grounded on the kinetic parameters, is presented. The method is applied to the kinetic study of the primary crystallization of Te in an amorphous alloy of nominal composition Ga20Te80, obtained by rapid solidification.
dc.format 10 p.
dc.format application/pdf
dc.language eng
dc.publisher Materials Research Society
dc.relation Reproducció del document publicat a: http://dx.doi.org/10.1557/JMR.1998.0094
dc.relation Journal of Materials Research, 1998, vol. 13, p. 744-753
dc.relation http://dx.doi.org/10.1557/JMR.1998.0094
dc.rights (c) Materials Research Society, 1998
dc.rights info:eu-repo/semantics/openAccess
dc.source Articles publicats en revistes (Física Quàntica i Astrofísica)
dc.subject Calorimetria
dc.subject Cristal·lització
dc.subject Cinemàtica
dc.subject Calorimetry
dc.subject Crystallization
dc.subject Kinematics
dc.title Accuracy in the experimental calorimetric study of the crystallization kinetics and predicitve transformation diagrams: Application to a Ga-Te amorphous alloy
dc.type info:eu-repo/semantics/article
dc.type info:eu-repo/semantics/publishedVersion


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